From Filter paper dropping test (Fig II) each and every
stage of dyeing shows that precipitation is there after using 1 gram per liter
sequestering agent (local also). It clearly shows precipitation starts from
salt stage (minor) at soda + caustic soda stage (maximum precipitation) in lab
stage.

Fig IIIFilter paper dropping test we have used glycerin in
dye dissolving then also dye precipitation was observed from salt (Minor) at
fixation stage (Maximum precipitation).

Fig IV-Filter paper dropping test used local sequestering
agent in dye dissolving also then also dye precipitation was observed.
Finally (local) Reactive Red SYG was replaced by
polyfunctional reactive dye (From colourtex) recipe was: M/C=50 KG-
Cora fix Rubine GDN (colourtex); -2.52% owf.
Reactive Yellow RD (local): -1.6% owf
Reactive N. Blue SGL (local): -0.14% owf
Common salt=80 gram per liter, soda ash=5 gram per
litre+caustic soda=1 gram per liter.
Process: -Dyesalt----sodas exhaust process (60 degree
Celsius dyeing temperature).
In Bulk trail dye was dissolved with (local) wetting agent
+sequestering agent (local) along with warm water (50 Degree Celsius). Then in
machine before addition of dye sequestering agent (1 gram per litre) was used
also.
Process: sequestering agent (1 gpl), room temp, 20 minute
running------Dissolved dye added slowly--- Common salt(II installment),40 degree
Celsius---temp rise to 60 degree Celsius(1 Degree rise in temperature)60
degree Celsius ,30 minute holding time----dissolved soda ash in two installment
at 15 minute gap---60 minute holding timebefore caustic soda addition check
samplecaustic soda in two installment---shade ok draincold
washneutralizationsoap (at boil,20 minute)hot wash(2)cold washcheck sample
for rubbing fastness checking
Fig V-shows bulk trail of each and every stage of dyeing no
precipitation was observed (Filter paper dropping test).
Fig VI:-shows wet rubbing fastness improvement observation
(ISO-X12) in yarn stage then after weaving stage (patti) along with regular
running process (yarn).
Wet rubbing fastness=3(ISO-X12).

Conclusion
Dye dissolving in wetting agent plus sequestering agent
shows uniformity from each and every stage of dyeing (See filter paper dropping
test Fig V)
Note: The readers are requested to take trial in first in laboratory then go
for bulk trial. This article is written in good faith for problem solving
attitude.
About the Author:
The author is working with Colourtex Industries Ltd. Surat
as the Product Manager for Reactive Dyes.
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